Pan-European solid-state NMR Infrastructure for Chemistry-Enabling Access

Badoni, S.; Berruyer, P.; Emsley, L., "Optimal Sensitivity for 1H Detected Relayed DNP of Organic Solids at Fast MAS"
J. Magn. Reson
DOI: 10.1016/j.jmr.2 024.107645
Open access: https://pubs.acs.org/doi/epdf/10.1021/acs.jpca.4c02452?ref=article
Raw data: https://pubs.acs.org/doi/10.1021/acs.jpca.4c02452?goto=supporting-info

S. Badoni, P. Berruyer, L. Niccoli, A. Lesage and L. Emsley, "Maximizing Relayed H Hyperpolarization Transfer by Slow-Fast MAS NMR Spectroscopy"
J. Phys. Chem. A Vol.128, 7005-7012
DOI: 10.1021/acs.jpca.4c02452
Open access: https://pubs.acs.org/doi/epdf/10.1021/acs.jpca.4c02452?ref=article
Raw data: https://pubs.acs.org/doi/10.1021/acs.jpca.4c02452?goto=supporting-info

Venkatesh, A.; Casano, G.; Wei, R.; Rao, Y.; Lingua, H.; Karoui, H.; Yulikov, M.; Ouari, O.; Emsley, L, "Rational Design of Dinitroxide Polarizing Agents for Dynamic Nuclear Polarization to Enhance Overall NMR Sensitivity"
Angew. Chem. Int. Ed. Engl
DOI: doi.org/10.1002 /anie.20231733 7
Open access: https://onlinelibrary.wiley. com/doi/10.1002/anie.202 317337
Raw data: https://zenodo.org/doi /10.5281/zenodo.1047 2538

Bastos, R., Marín-Montesinos, I., Ferreira, S.S., Mentink-Vigier, F., Sardo, M., Mafra, L., Coimbra, M.A., Coelho, E., "Covalent connectivity of glycogen in brewer’s spent yeast cell walls revealed by enzymatic approaches and dynamic nuclear polarization NMR"
Carbohydrate Polymers
DOI: 10.1016/j.carbpol.2023.121475
Open access: https://www.sciencedirect.com/science/article/pii/S0144861723009402
Raw data: https://zenodo.org/records/14000959

Torodii, D., Holmes, J.B., Moutzouri, P., et al, "Crystal structure validation of verinurad via proton-detected ultra-fast MAS NMR and machine learning"
Faraday Discuss
DOI: 10.1039/D4FD00076E
Open access: https://pubs.rsc.org/en/content/articlepdf/2024/fd/d4fd00076e
Raw data: https://doi.org/10.24435/materialscloud:qk-x9

Miao, Z; Scott, F. J, Van Tol, J; Bowers, C. R; Veige, A. S; F. Mentink-Vigier, "Soliton Based Dynamic Nuclear Polarization: An Overhauser Effect in Cyclic Polyacetylene at High Field and Room Temperature"
J. Phys. Chem. Lett Vol.15, 3369-3375, 12
DOI: 10.1021/acs.jpclett.3c03591
Open access: https://pubs.acs.org/doi/10.1021/acs.jpclett.3c03591
Raw data: https://zenodo.org/records/14645908

Koppe. J; Sanders. K; Robinson. T; Lejeune. A; Proriol. A; Wegner. S; Purea. A; Engelke. F; Clément. R; Grey. C; Pell. A; Pintacuda. G, "Resolving Structures of Paramagnetic Systems in Chemistry and Materials Science by Solid-State NMR: the Revolving Power of Ultra-Fast MAS"
Angewandte Chemie International Edition Vol.64, , 1
DOI: 10.1002/anie.202408704
Open access: https://doi.org/10.1002/anie.202408704
Raw data: https://zenodo.org/records/11120901

Steinberg, Y., Sebti, E., Moroz, I.B., et al., "Composition and Structure of the solid electrolyte interphase on Na-Ion Anodes Revealed by Exo- and Endogenous Dynamic Nuclear Polarization─NMR Spectroscopy"
J. Am. Chem. Soc
DOI: 10.1021/jacs.4c06823
Open access: https://pubs.acs.org/doi/10.1021/jacs.4c06823
Raw data: https://doi.org/10.34933/46bd9e52-9e84-4c02-bb5e-e332a6296a7d

Holmes, J.B., Torodii, D., Balodis, M., Cordova, M., Hofstetter, A., Paruzzo, F., Lill, S.O.N., Eriksson, E., Berruyer, P., Almeida, B.S. de, Quayle, M., Norberg, S., Ankarberg, A.S., Schantz, S., Emsley, L, "Atomic-level structure of the amorphous drug atuliflapon via NMR crystallography"
Chem. Sci
DOI: 10.1039/D4FD00078A
Open access: https://pubs.rsc.org/en/content/articlelanding/2024/fd/d4fd00078a
Raw data: https://doi.org/10.24435/materialscloud:9r-b9

Torodii, D.; Holmes, J. B.; Grohe, K.; De Oliveira-Silva, R.; Wegner, S.; Sakellariou, D.; Emsley, L. , "Observation of 1H-1H J-Couplings in Fast Magic-Angle-Spinning Solid-State NMR Spectroscopy"
Nat Commun Vol.15, 10799, 1
DOI: 10.1038/s41467-024-55126-9.
Open access: https://www.nature.com/articles/s41467-024-55126-9
Raw data: https://zenodo.org/records/14186568